- Title
- Ionic liquids accelerate access to N-substituted-1,8-naphthalimides
- Creator
- MacGregor, Kylie A.; McCluskey, Adam
- Relation
- Tetrahedron Letters Vol. 52, Issue 7, p. 767-769
- Publisher Link
- http://dx.doi.org/10.1016/j.tetlet.2010.12.015
- Publisher
- Elsevier
- Resource Type
- journal article
- Date
- 2011
- Description
- The synthesis of N-substituted-1,8-naphthalimides is accelerated in the presence of the room temperature ionic liquid [BMIM][NO₃]. Reaction times are reduced from 18 h in volatile organic compounds (VOCs) (PhCH₃, EtOH and THF) to 20 min in the ionic liquid [BMIM][NO₃]. The reaction yields are typically increased to >85% and the products are isolated by ethanol-mediated precipitation direct from the ionic liquid, requiring no further purification.
- Subject
- room temperature ionic liquids; 1,8-Naphthalimides; focused libraries; [BMIM][NO₃]
- Identifier
- http://hdl.handle.net/1959.13/1065909
- Identifier
- uon:17953
- Identifier
- ISSN:0040-4039
- Language
- eng
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